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This book has arisen from a series of lectures developed by Dr Gillan McMahon and delivered to students on the taught postgraduate module on instrumentation at Dublin City University. Gillian was previously herself a student in DCU and since graduating, she has developed her analytical background initially in industry in the pharmachem arena, and more recently, as a very successful academic teacher and researcher. She gained a wealth of experience over a broad range of analytical techniques in the pharmachem industry, working with the Geotest Chemical Company (USA), Newport Pharmaceuticals (Ireland), Bristol-Myers Squibb (Ireland) and Zeneca Pharmaceuticals (UK). This experience applied not just to the use of techniques and methods, but also to data tracking and compliance, which is a critical aspect for this sector. While with BMS, she was engaged in training of staff in advanced analytical techniques and compliance at other sites in Italy and Puerto Rico prior to production campaigns.